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粉末注射成形制备薄壁Al2O3–B4C环形芯块

Preparation of Al2O3–B4C thin-wall tube pellet by powder injection molding

  • 摘要: 使用多组元蜡基粘结剂,通过粉末注射成形工艺,结合溶剂脱脂和热脱脂,成功烧结制备出壁厚为0.7 mm的近净尺寸环形Al2O3–B4C薄壁管。结果表明,当石蜡占粘结剂质量分数45%时,喂料具有较低的黏度和较好的抗弯强度;当固相体积分数为58%时,喂料在保证低黏度的前提下具有良好性能。当烧结温度在1550 ℃至1650 ℃范围内时,芯块相对密度及抗弯强度随温度上升而增高;当烧结温度达到1650 ℃时,芯块的密度及强度有所下降,芯块密度随B4C粒度增大而增大,抗弯强度随粒度增大先增大后减小。

     

    Abstract: The annular Al2O3–B4C thin wall tube with the wall thickness of near 0.7 mm was successfully sintered by powder injection molding combined with the solvent degreasing and thermal degreasing, using the multi-component wax-based binder. The results show that, when the paraffin mass fraction is 45%, the feedstock has the lower viscosity and the better bending strength. When the solid phase volume fraction is 58%, the feedstock has the good performance in the premise of low viscosity. When the sintering temperature is in the range of 1550 ℃ to 1650 ℃, the relative density and the bending strength of the pellets increase with the increase of temperature. When the sintering temperature reaches 1650 ℃, the density and strength of the pellets begin to decrease slightly, the density increases with the increase of the B4C particle size, and the bending strength increases first and then decreases with the increase of particle size.

     

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