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粉末预处理对钨坩埚应用性能的影响

Effect of powder pretreatment on the application performance of tungsten crucible

  • 摘要: 利用不同原料粉末制备钨坩埚样品,并于高温环境下进行应用模拟实验。结果表明,射流分级预处理有助于提升钨坩埚组织均匀性及整体性能;以费氏粒度3.0~3.5 μm的钨粉为原料,经射流分级、压制、烧结等工艺,可制得密度较高(18.770 g·cm−3)、维氏硬度较高(HV0.3 372.15)的钨制品;将该钨坩埚置于高温环境下进行模拟应用验证,其密度及微观形貌较为稳定,变化较小。

     

    Abstract: The tungsten crucible samples were prepared by using the different tungsten powders, and the application simulation experiment was carried out in high temperature environment. The results show that, the jet grading pretreatment technology is an efficient process to improve the qualities of the tungsten crucible. The tungsten products with high density (18.770 g·cm−3) and high Vickers hardness (HV0.3 372.15) are prepared by jet grading, pressing, and sintering, using the tungsten powders with the Feller size of 3.0~3.5 μm as the raw materials. Meanwhile, the simulation application of tungsten crucibles is verified in the high temperature environment, which shows that the density and microstructure are stable.

     

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