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郭秋实. 高密度钨合金粉末的离心喷雾造粒工艺研究[J]. 粉末冶金技术. DOI: 10.19591/j.cnki.cn11-1974/tf.2021070009
引用本文: 郭秋实. 高密度钨合金粉末的离心喷雾造粒工艺研究[J]. 粉末冶金技术. DOI: 10.19591/j.cnki.cn11-1974/tf.2021070009
Study on the Centrifugal Spray Granulator Process for Tungsten Heavy Alloy Powder[J]. Powder Metallurgy Technology. DOI: 10.19591/j.cnki.cn11-1974/tf.2021070009
Citation: Study on the Centrifugal Spray Granulator Process for Tungsten Heavy Alloy Powder[J]. Powder Metallurgy Technology. DOI: 10.19591/j.cnki.cn11-1974/tf.2021070009

高密度钨合金粉末的离心喷雾造粒工艺研究

Study on the Centrifugal Spray Granulator Process for Tungsten Heavy Alloy Powder

  • 摘要: 针对模压用高密度钨合金粉末,研究了离心式喷雾造粒工艺参数对造粒粉末特性的影响。结果表明,料浆的固含量和动力粘度,喷雾时的进出口温度、进料速度和雾化盘转速对高密度钨合金造粒粉的松装密度、流速、粒度分布和造粒粉的形貌均会造成显著的复杂的影响。研究获得了一组优化的工艺参数:料浆的固含量为70%(体积百分比为9.7%),料浆动力粘度为2.5 Pa?s,雾化塔进口温度为300 ℃,出口温度为120 ℃,蠕动泵进料速度为90 mL?min-1,雾化盘转速为9800 r?min-1,该工艺参数下制备的造粒粉性能良好,粒度分布范围狭窄,造粒粉的D50为52 μm、D90为91 μm,且粉末流速为14.4 s?(50g)-1,流动性好。

     

    Abstract: For the development of ready to press powder of tungsten heavy alloy, the influences of process parameters of centrifugal spray granulation were investigated. The results showed that the bulk density, flow rate, particle size distribution and morphology of granulated powder were significantly influenced by the solid loading and dynamic viscosity of slurry, inlet and outlet temperature, feed rate and rotational speed of atomizer disk. A set of process parameters were obtained included the solid loading of 70%(volume percentage is 9.7%) and dynamic viscosity of 2.5 Pa?s for the slurry, the inlet and outlet temperatures of 300 ℃ and 120 ℃ respectively, the feeding rate 90 mL?min-1 of peristaltic pump , and the rotational speed 9800 r?min-1 of atomizer disk. The proper granulated powder with good flowability and narrow particle size distribution can be obtained by using these parameters, the D50 and D90 of granulation powder are 52 μm and 91 μm respectively, and the flow rate is 14.4 s?(50g)-1.

     

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