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刘兴刚, 刘珂, 马召俊, 张德良. 固态再生H11钢退火后的微观组织与力学性能分析[J]. 粉末冶金技术. DOI: 10.19591/j.cnki.cn11-1974/tf.2021120010
引用本文: 刘兴刚, 刘珂, 马召俊, 张德良. 固态再生H11钢退火后的微观组织与力学性能分析[J]. 粉末冶金技术. DOI: 10.19591/j.cnki.cn11-1974/tf.2021120010
Analysis of microstructure and mechanical properties of solid-state recycled H11 steel after annealing[J]. Powder Metallurgy Technology. DOI: 10.19591/j.cnki.cn11-1974/tf.2021120010
Citation: Analysis of microstructure and mechanical properties of solid-state recycled H11 steel after annealing[J]. Powder Metallurgy Technology. DOI: 10.19591/j.cnki.cn11-1974/tf.2021120010

固态再生H11钢退火后的微观组织与力学性能分析

Analysis of microstructure and mechanical properties of solid-state recycled H11 steel after annealing

  • 摘要: 前期研究H11车削屑固态再生钢时发现,车削屑研磨获得的不同粒度粉末经压坯和挤压锻工艺后制备的实验钢韧性较差,本文研究H11钢车削屑固态再生的最优的等温球化退火热处理工艺对微观组织和力学性能的影响。工艺条件包括10 ℃/min的速度从室温升温至880 ℃,保温3 h,随炉冷却至750 ℃,保温4 h,随炉冷却至550 ℃后出炉空冷。对热处理后的样品进行力学性能测试、以及XRD和SEM微观素质观察等表征。发现等温球化退火处理后实验钢的组织为球状珠光体和弥散分布的颗粒状碳化物;材料的塑性变好,延伸率从3.4 %升高到12.8 %,但抗拉强度和硬度下降;粉末粒度影响H11车削屑固态再生钢在高温挤压锻后的强韧性,粒度越小,高温挤压锻后氧化越严重,强韧性就越差。

     

    Abstract: In the previous study on the H11 steel fabricated by thermomechanical consolidation of powders made from grinding turning chips, it was found that the toughness of the experimental steel prepared with the powders of different particle sizes was poor. This paper studies the effect of annealing heat treatment on microstructure and mechanical properties of the consolidated steel. The heat treatment involves heating from room temperature to 880 °C at a rate of 10 °C/min, holding for 3 h, cooling in the furnace to 750 °C, holding for 4 h, cooling in the furnace to 550 °C and then air cooling. The mechanical property test, and XRD and SEM observations show the following findings. After the isothermal spheroidizing annealing treatment, the microstructure consists of spherical pearlite and dispersed granular carbide particles. The ductility of the material becomes better with the elongation to fracture increasing from 3.4 % to 12.8 % after the heat treatment, but the tensile strength and hardness decrease. The powder particle size affect the strength and toughness of consolidated H11 steel. The smaller the particle size, the more severe the oxidation after high temperature extrusion forging, and the worse the strength and toughness.

     

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