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热等静压温度对Mo2FeB2基金属陶瓷涂层组织及性能的影响

Effect of hot isostatic pressing temperature on the microstructure and properties of Mo2FeB2-based cermets coatings

  • 摘要: 通过热等静压工艺在06Cr13Ni4Mo不锈钢基体上制备Mo2FeB2金属陶瓷涂层,研究了热等静压温度对涂层组织及性能的影响。结果表明:Mo2FeB2基金属陶瓷涂层主要由硬质相、粘结相和过渡相组成,并存在少量孔洞,其中硬质相主要为Mo2FeB2陶瓷强化相,粘结相主要为Fe,过渡相以Fe–Ni为主。随着热等静压温度升高,涂层组织从大块硬质相+粘结相逐渐转变为均匀细小的硬质相,热等静压后的涂层硬度均大于HV 1100。热等静压温度升高增强了界面元素扩散能力,当温度达到1150 ℃时,界面过渡层消失。06Cr13Ni4Mo基体材料的强度和硬度随着热等静压温度升高有所降低,塑性和冲击功提升。

     

    Abstract: Mo2FeB2-based cermet coatings were prepared on 06Cr13Ni4Mo steels by hot isostatic pressing (HIP) process, and the effects of HIP temperatures on the microstructures and mechanical properties of the Mo2FeB2-based cermet coatings were studied. The results show that the coatings are mainly composed of hard phase (Mo2FeB2), bonded phase (Fe), and transition phase (Fe–Ni) with a small number of pores. With the HIP temperature increases, the coatings gradually transform from the hard phases and bonding phases to the uniform and small hard phases, and all of the coating hardness are greater than HV 1100. For the interfacial transition layers, with the increase of HIP temperature, the element diffusion ability is improved; when the temperature reaches 1150 ℃, the interfacial transition layer disappears. As the same time, the strength and hardness of the 06Cr13Ni4Mo stainless steel matrix are reduced, while the plasticity and impact energy increase.

     

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