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铜粉形貌与烧结温度对MIM多孔铜组织及性能的影响

Effects of Copper Powder Morphology and Sintering Temperature on the Microstructure and Properties of MIM-fabricated Porous Copper

  • 摘要: 本文以不同形貌(近球状、不规则状和团簇状)的铜粉为原料,采用金属注射成形与粉末烧结技术相结合制备多孔结构试样。研究铜粉形貌及烧结温度对烧结试样的孔隙特征、吸水性能及力学性能的影响。结果表明:在相同烧结温度下,团簇状铜粉制备试样的孔隙率最高,而近球状粉制备试样的孔隙率最低。相应的,近球状粉制备试样在各烧结温度下表现出最小的体积收缩率。随烧结温度由850 ℃提升至1000 ℃,团簇状铜粉制备试样的孔隙率由44.3 %下降至20.5 %,其吸水速度由1.2 mm/s降至0.5 mm/s。在力学性能方面,近球形粉在各烧结温度下均表现出最好的抗拉强度。随烧结温度由850 ℃提升至1000 ℃,近球状粉制备试样的抗拉强度由8.7 MPa提高至117.6 MPa。

     

    Abstract: In this study, porous copper material was prepared from copper powders with different morphologies (near-spherical, irregular, and cluster-like) by combining metal injection molding and powder sintering technologies. The effects of power morphology and sintering temperature on the pore features, water absorption and mechanical properties of the sintered samples were studied. The results showed that at the same sintering temperature, the samples prepared from cluster-like copper powder exhibited the highest porosity, while those prepared from near-spherical powder had the lowest porosity. Correspondingly, samples prepared from near-spherical powder displayed the minimum volume shrinkage rate at all sintering temperatures. As the sintering temperature increased from 850 ℃ to 1000 ℃, the porosity of the samples prepared from cluster-like copper powder decreased from 44.3% to 20.5%. And their water absorption rate drops from 1.2 mm/s to 0.5 mm/s. In terms of mechanical properties, the tensile strength of samples prepared from copper powders with different morphologies all increased with the rising sintering temperature. Among them, the near-spherical powder showed the best tensile strength at all sintering temperatures. With the sintering temperature increasing from 850 ℃ to 1000 ℃, the tensile strength of the samples prepared from near-spherical powder increased from 8.7 MPa to 117.6 MPa.

     

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