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固溶处理对粉-管结合阵列多孔钢压缩性能的影响

Effect of solution treatment on compressive properties of powder-tube bonded array porous steels

  • 摘要: 针对传统烧结多孔钢孔隙分布随机、应力集中严重、吸能稳定性差等问题,采用球形316L不锈钢粉末与薄壁316L钢管阵列,通过粉末-管冶金结合免造孔剂烧结工艺制备粉-管结合阵列多孔钢,研究不同保温时间固溶处理对其物相演变、显微组织及各向异性压缩性能的影响。结果表明:烧结态试样析出σ相与M23C6富Cr第二相,造成基体C贫化,劣化压缩性能;1050 ℃固溶处理可促使富Cr第二相回溶于奥氏体基体,保温30 min时第二相基本完全溶解,继续延长保温至45 min、60 min会发生第二相复析。粉-管冶金结合阵列结构结合适度固溶处理可有效改善多孔钢的压缩承载与能量吸收性能。该多孔钢表现显著压缩各向异性,面外压缩承载与吸能能力优于面内压缩。1050 ℃固溶30 min试样综合压缩性能最优,面内压缩平台应力、总吸能、比吸能较烧结态分别提升51.04%、31.92%、25.00%;面外压缩上述指标分别提升40.65%、55.24%、30.85%。

     

    Abstract: Aiming at the drawbacks of conventionally sintered porous steels, such as random pore distribution, severe stress concentration, and poor energy-absorption stability, the powder-tube bonded array porous steels were fabricated by additive-free sintering using spherical 316L stainless steel powders and thin-walled 316L steel tubes. The effects of solution treatment with different holding time on phase evolution, microstructure, and anisotropic compressive properties were investigated. The results show that, the σ phase and Cr-rich M23C6 secondary phases precipitate in as-sintered specimens, leading to Cr depletion in austenite matrix and compressive performance deterioration. Solution treatment at 1050 ℃ promotes the re-dissolution of Cr-rich secondary phases into austenite matrix. The secondary phases are almost completely dissolved at the holding time of 30 min, whereas the re-precipitation occurs when holding time further increases to 45 min and 60 min. The powder-tube metallurgically bonded array structure combined with appropriate solution treatment can effectively improve the compressive load-bearing and energy-absorption performance of porous steel. The prepared porous steels exhibit the obvious compressive anisotropy, and the load-bearing and energy-absorption capacities under out-of-plane compression are superior to those under in-plane compression. The specimen solution-treated at 1050 ℃ for 30 min achieves the optimal comprehensive compressive properties. Compared with the as-sintered samples, the plateau stress, total energy absorption, and specific energy absorption under in-plane compression increase by 51.04%, 31.92%, and 25.00%, respectively; the corresponding increments under out-of-plane compression are 40.65%, 55.24%, and 30.85%.

     

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