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调控工艺参数实现真空热压CPM10V工模具钢中所有区域完全致密化

Manipulation of processing parameters towards full densification in all regions of vacuum hot-pressed CPM10V steel

  • 摘要: 为提高真空热压高合金工模具钢在模具/粉末界面区域的致密化程度,本文以CPM10V钢为实验材料,研究了提高该区域致密度的工艺方法。实验结果表明,提高热压压力或温度均可使热压的CPM10V钢在石墨模具侧壁附近区域(即热压工具钢的外侧面附近)达到近乎完全致密化。具体而言,在1150 ℃下热压压力从30 MPa提高到50MPa后,热压 CPM10V钢下层边缘区域的相对密度从98.49 ± 0.11%提高到99.18 ± 0.11%,这是因为提高压制压力可以使处于模具侧壁附近的粉末受到的净压力(压制压力减去摩擦应力)得到提高,从而提高净压力与粉末流变应力的比值。另一方面,在30 MPa下热压温度从1150 ℃提高到1180 ℃后,热压CPM10V钢下层边缘区域的相对密度从98.49 ± 0.11%提高到99.05 ± 0.06%,由于提高压制温度可以降低粉末的流变应力,也提高了净压力与粉末流变应力的比值。上述两种工艺措施都增强粉末的塑性流动能力,使颗粒间的孔隙得到充分填充,从而实现CPM10V钢的近乎完全致密化。此外,实验结果表明,CPM10V钢外侧面附近的近乎完全致密化也提高了其力学性能(例如:硬度和弯曲断裂强度)。

     

    Abstract: Selecting CPM10V steel as a model material, the present work reports a study on processing routes to improve relative density in the vicinities of graphite mold sidewall in vacuum hot-pressed highly alloyed tool steels. The experimental results show that an increase in hot-pressing pressure or temperature promotes near-full densification in regions adjacent to the graphite mold sidewall, i.e., the outer surface of the hot-pressed steel. When the hot-pressing pressure was increased from 30 MPa to 50 MPa at 1150 ℃, the relative density in the lower sidewall region increased from 98.49 ± 0.11 % to 99.18 ± 0.11 %, which is likely attributed to an increase in net pressure and thus an increase in the ratio of net pressure to powder flow strength. In addition, when the hot-pressing temperature was increased from 1150 ℃ to 1180 ℃ at 30 MPa, the relative density in the same region increased from 98.49 ± 0.11 % to 99.05 ± 0.06 %, due to a decrease in powder flow strength, also resulting in an increase in the ratio of net pressure to powder flow strength with the same net pressure. In both cases, the increased ratio of net pressure to powder flow strength enhances powder plastic flow and facilitates the elimination of pores between powders, leading to near-full densification. As a result of the improved densification near the outer surface, mechanical properties (specifically, hardness and bending strength) of the hot-pressed CPM10V are enhanced.

     

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