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气体吸附法测定粉末比表面

DETERMINATION OF SPECIFIC SURFACE OF POWDERS BY GAS ADSORPTION METHOD

  • 摘要: 简要了静态法和动态法所采用的两类有代表性的仪器。实验表明,两类仪器所得结果是比较一致的。该方法所测量的比表面为总表面积。采用氮吸附质时,可采用单点法。测量小比表面时,应选用低饱和蒸汽压的吸附质,如氩气、氪气等,采用不同的吸附质,所得结果一致。采用氪吸附质,可测量的最小比表面为0.001m2/g。

     

    Abstract: The paper has outlined two kinds of typical apparatus used for static and dynamic methods. The results obtained by two kinds of apparatus are comparatively consistent. The specific surface measured by this method is total surface area. In case of the use of nitrogen adsorbate, single point method can be adopted. In case of the measure of small specific surface, the adsorbate with low saturation vapour pressure should be shosen, e. g. argon, krypton, etc.. Consistent results have been obtained by adopting different adsorbates. A minimum specific surface of 0.001m2/g can be measured by using krypton adsorbate.

     

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