Synthesis of MoO3 Nanobelts /RGO by One-Step Hydrothermal Process and its Electrochemical Properties
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摘要: 为了提高三氧化钼(MoO3)作为超级电容器电极材料的储能性能,通过一步水热法合成了MoO3纳米带/RGO复合材料,探索了水热法对复合材料的组织结构及电化学性能的影响。利用X射线衍射分析、扫描电子显微形貌、傅里叶变换红外光谱分析、循环伏安、恒流充放电等技术对材料的物相和形貌以及电化学性能进行了表征和分析。结果显示,通过一步水热法成功制得MoO3纳米带/RGO复合材料,复合前MoO3比电容为228 F.g-1,复合后比电容提高了17.5%。复合材料中MoO3纳米带被RGO包裹或者附着在RGO表面,增强了材料的导电性并使其结构更稳定,从而提升了电化学性能。
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关键词:
Abstract: To improve the energy storage performance of MoO3 as a supercapacitor electrode material,MoO3/RGO composites were synthesized by one-step hydrothermal process. The phase structure, morphology and electrochemical properties of the materials were characterized by XRD, SEM, FTIR, cyclic voltammetry, constant current charge discharge, and the effect of hydrothermal process on the microstructure and electrochemical properties of the composites was explored. The results showed that the MoO3 nanoribbons/RGO composites were successfully fabricated by a one-step hydrothermal method. Encouragingly, the specific capacitance of composite material was increased by 17.5% compared with that of pure MoO3 (228 F.g-1). Furthermore, the MoO3 nanoribbons were wrapped by RGO or attached to the surface of RGO in the composite, which induced obvious enhancement of the electrical conductivity as well as the structure stability, and subsequently the ultimate electrochemical properties of the original materials.-
Key words:
- molybdenum trioxide /
- hydrothermal method /
- graphene oxide /
- supercapacitor /
- specific capacitance
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