Citation: | REN Daya, ZAN Xiang. Damage and microstructure evolution of yttria particle reinforced tungsten plates under laser thermal shock[J]. Powder Metallurgy Technology, 2024, 42(3): 304-311. DOI: 10.19591/j.cnki.cn11-1974/tf.2022030016 |
Yttria particle reinforced tungsten plates with different thickness reduction were prepared by powder metallurgy technology combined with rolling process. The prepared samples with different recrystallization volume fractions were subjected to transient laser thermal shock experiments to study the surface damage and microstructure evolution under the synergistic effect of recrystallization caused by long-term steady-state heat load and transient thermal shock. In the results, the cracks, melting, and other damages occur on the sample surface because of the thermal shock loading. Moreover, the recrystallization process would accelerate the widening of cracks and the enlargement of melting area, which greatly reduces the ability of the materials to resist transient heat loading. Under the same power density, the damage level of the samples with 67% thickness reduction is obviously lower than that with 50% thickness reduction, and the former has better thermal shock resistance; the molten zones of these two samples are composed by the columnar grains, which are associated with the grain size of the initial matrix below, and the columnar grains formed in rolled samples are finer and numerous, while those of the fully recrystallized samples are coarser.
[1] |
杨毅超, 李延超, 李雅馨, 等. 磁控核聚变装置中钨基合金面向等离子体材料的研究现状与进展. 中国钨业, 2020, 35(6): 72 DOI: 10.3969/j.issn.1009-0622.2020.06.010
Yang Y C, Li Y C, Li Y X, et al. Present situation and research progress of tungsten-based alloy plasma-facing materials in magnetron nuclear fusion devices. China Tungst Ind, 2020, 35(6): 72 DOI: 10.3969/j.issn.1009-0622.2020.06.010
|
[2] |
罗来马, 颜硕, 刘祯, 等. 面向等离子体材料用先进钨复合材料的改性研究进展与趋势. 粉末冶金技术, 2023, 41(1): 12
Luo L M, Yan S, Liu Z, et al. Research progress and trend of advanced tungsten composite modification used for plasma facing materials. Powder Metall Technol, 2023, 41(1): 12
|
[3] |
Linke J, Du J, Loewenhoff T, et al. Challenges for plasma-facing components in nuclear fusion. Matter Radiat Extrem, 2019, 4(5): 056201 DOI: 10.1063/1.5090100
|
[4] |
Van den Kerkhof S, Blommaert M, Pitts R A, et al. Impact of ELM mitigation on the ITER monoblock thermal behavior and the tungsten recrystallization depth. Nucl Mater Energy, 2021, 27: 101009 DOI: 10.1016/j.nme.2021.101009
|
[5] |
Okita T, Matsuda Y, Saito S, et al. Observation of surface deformation of tungsten exposed to single pulsed high heat flux and magnetic field for divertor design. Fusion Eng Des, 2021, 171: 112547 DOI: 10.1016/j.fusengdes.2021.112547
|
[6] |
种法力, 陈俊凌, 郑学斌. 核聚变等离子体喷涂钨涂层瞬态高热负荷损伤行为. 特种铸造及有色合金, 2017, 37(3): 313
Zhong F L, Chen J L, Zheng X B. Transient high heat loading performance of plasma sprayed tungsten coating for fusion device. Spec Cast Nonferrous Alloys, 2017, 37(3): 313
|
[7] |
Zhao B L, Xia Y P, Zhang L F, et al. Effects of rolling reduction on microstructural evolution and mechanical properties of W–0.5wt%ZrC alloys. Mater Sci Eng A, 2022, 830: 142310 DOI: 10.1016/j.msea.2021.142310
|
[8] |
Shi J, Luo L M, Wang S, et al. Preparation of TiC-doped W–Ti alloy and heat flux performance test under laser beam facility. Fusion Eng Des, 2018, 126: 79 DOI: 10.1016/j.fusengdes.2017.11.026
|
[9] |
Wang J F, Zuo D W, Zhu L, et al. Effects and influence of Y2O3 addition on the microstructure and mechanical properties of binderless tungsten carbide fabricated by spark plasma sintering. Int J Refract Met Hard Mater, 2018, 71: 167 DOI: 10.1016/j.ijrmhm.2017.11.016
|
[10] |
陈铮, 杨军军, 章林, 等. La2O3掺杂纳米W粉致密化行为与性能. 粉末冶金技术, 2021, 39(5): 387
Chen Z, Yang J J, Zhang L, et al. Densification behavior and performance of La2O3-doped W nanopowders. Powder Metall Technol, 2021, 39(5): 387
|
[11] |
Lian Y, Liu X, Feng F, et al. Mechanical properties and thermal shock performance of W–Y2O3 composite prepared by high-energy-rate forging. Phys Scr, 2017, T170: 014044 DOI: 10.1088/1402-4896/aa8f2d
|
[12] |
Lü Y Q, Han Y, Zhao S Q, et al. Nano-in-situ-composite ultrafine-grained W–Y2O3 materials: Microstructure, mechanical properties and high heat load performances. J Alloys Compd, 2021, 855: 157366 DOI: 10.1016/j.jallcom.2020.157366
|
[13] |
昝祥, 孙海涛, 吴玉程, 等. 一种具有优异热稳定性的钨–氧化钇复合材料的加工方法: 中国专利, CN111334679A. 2021-11-30
Zan X, Sun H T, Wu Y C, et al. A Processing Method of Tungsten Yttria Oxide Composite with Excellent Thermal Stability: China Patent, CN111334679A. 2021-11-30
|
[14] |
Zan X, Gu M, Wang K, et al. Recrystallization kinetics of 50% hot-rolled 2% Y2O3 dispersed tungsten. Fusion Eng Des, 2019, 144: 1 DOI: 10.1016/j.fusengdes.2019.04.017
|
[15] |
孙海涛. 氧化钇颗粒增强轧制钨板再结晶行为及其对辐照损伤的影响研究[学位论文]. 合肥: 合肥工业大学, 2021
Sun H T. Study on Recrystallization Behavior of Yttrium Oxide Particle-Reinforced Rolled Tungsten Plates and the Effect on Irradiation Damage [Dissertation]. Hefei: Hefei University of Technology, 2021
|
[16] |
Hirai T, Pintsuk G, Linke J, et al. Cracking failure study of ITER-reference tungsten grade under single pulse thermal shock loads at elevated temperatures. J Nucl Mater, 2009, 390-391: 751 DOI: 10.1016/j.jnucmat.2009.01.313
|
[17] |
Matsuda Y, Yamashita S, Miyamoto Y, et al. In-situ measurement of surface modifications of tungsten exposed to pulsed high heat flux for divertor design in tokamak-type fusion nuclear reactors. Fusion Eng Des, 2020, 161: 112042 DOI: 10.1016/j.fusengdes.2020.112042
|