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Volume 37 Issue 3
Jan.  2021
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ZHANG Wang-nian, WANG Xin-hai, WANG Li-fang, XU Huan, YANG Sheng-dao, LI Yong-jie, HU Ze-hao. Effect of Fe2O3 additive agent on sintering properties of CaZrO3 ceramics[J]. Powder Metallurgy Technology, 2019, 37(3): 220-224. DOI: 10.19591/j.cnki.cn11-1974/tf.2019.03.010
Citation: ZHANG Wang-nian, WANG Xin-hai, WANG Li-fang, XU Huan, YANG Sheng-dao, LI Yong-jie, HU Ze-hao. Effect of Fe2O3 additive agent on sintering properties of CaZrO3 ceramics[J]. Powder Metallurgy Technology, 2019, 37(3): 220-224. DOI: 10.19591/j.cnki.cn11-1974/tf.2019.03.010
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Effect of Fe2O3 additive agent on sintering properties of CaZrO3 ceramics

  • School of Mechanical and Materials Engineering, Jiujiang University, Jiujiang 332005, China

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  • Corresponding author:

    ZHANG Wang-nian, E-mail:zwn2003@126.com

  • Received Date: July 25, 2018
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    • Abstract
  • Using analytical Ca(OH)2 and m-ZrO2 as the raw materials in the mole ratio of 1:1, the compacted cylinder samples of calcium zirconate (CaZrO3) ceramics in the dimension of ø20 mm × 20 mm were synthetized by sintering at 1600 ℃ for 3 h, adding the Fe2O3 powders in different mass fractions as the additive agent.The effects of Fe2O3 additive agent on sintering properties, phase composition, and microstructures of CaZrO3 ceramics were studied by apparent porosity density determinator, X-ray diffraction (XRD) diffractometer, and scanning electron microscope (SEM).The results show that, without the addition of Fe2O3, the sharking of CaZrO3 samples is 12.72%, the bulk density and apparent porosity of sintered CaZrO3 samples at 1600 ℃ are 3.92 g·cm-3 and 14.9%, respectively, and the grain size of CaZrO3 is only 4.22 μm.With the addition of Fe2O3 in mass fraction of 0.75%, the sharking of CaZrO3 samples is 17.20%, the bulk density and apparent porosity of sintered CaZrO3 samples at 1600 ℃ are 4.68 g·cm-3 and 6.8%, respectively, and the grain size of CaZrO3 reaches to 5.21 μm.
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    • References (13)
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