AdvancedSearch
JIANG Shan, LI Jie, CHEN Yao. Study on microstructure and properties of tungsten alloy prepared by laser sintering[J]. Powder Metallurgy Technology, 2020, 38(5): 344-349. DOI: 10.19591/j.cnki.cn11-1974/tf.2019060004
Citation: JIANG Shan, LI Jie, CHEN Yao. Study on microstructure and properties of tungsten alloy prepared by laser sintering[J]. Powder Metallurgy Technology, 2020, 38(5): 344-349. DOI: 10.19591/j.cnki.cn11-1974/tf.2019060004

Study on microstructure and properties of tungsten alloy prepared by laser sintering

More Information
  • Corresponding author:

    JIANG Shan, E-mail: 382595277@qq.com

  • Received Date: June 16, 2019
  • The tantalum and rhenium doped tungsten-based alloys were prepared by laser sintering, and the microstructure and mechanical properties of the tungsten-based alloy samples were investigated by scanning electron microscope (SEM), optical microscope (OM), X-ray diffraction (XRD), and micro-hardness tester. The results show that, the laser power and laser scanning speed are the important factors affecting the relative density of tungsten alloy blocks, the compact tungsten alloy block materials are obtained by optimizing the parameters. The powder oxidation is avoided by the desorption and deoxygenation pretreatment and the inert gas protection. The microstructures show that, the static recrystallization occurs in the laser sintering process. The equiaxial grains with the significantly larger size than the powder grains are formed at the core of the tungsten-based alloy sample, and the equiaxial grains with the size slightly larger than the powder grains size are formed at the edge of the tungsten-based alloy sample. The XRD results show that, the doped tantalum element exists as the solid dissolved atoms in tungsten matrix. The performance testing results show that, the density decreases with the increase of tantalum, but the microhardness increases.
  • [1]
    余泽全, 刘良先. 2017年上半年中国钨品进出口分析. 中国钨业, 2017, 32(4): 1 DOI: 10.3969/j.issn.1009-0622.2017.04.001

    Yu Z Q, Liu L X. Import and export analysis of the tungsten products in China in the first half of 2017. China Tungsten Ind, 2017, 32(4): 1 DOI: 10.3969/j.issn.1009-0622.2017.04.001
    [2]
    刘良先, 余泽全. 2016年上半年中国钨品进出口分析. 中国钨业, 2016, 31(4): 1 DOI: 10.3969/j.issn.1009-0622.2016.04.001

    Liu L X, Yu Z Q. Import and export analysis of the tungsten products of China in the first half of 2016. China Tungsten Ind, 2016, 31(4): 1 DOI: 10.3969/j.issn.1009-0622.2016.04.001
    [3]
    刘良先, 余泽全. 2015年上半年中国钨品进出口分析. 中国钨业, 2015, 30(4): 1 DOI: 10.3969/j.issn.1009-0622.2015.04.001

    Liu L X, Yu Z Q. Import and export analysis of the tungsten products of China in the first half of 2015. China Tungsten Ind, 2015, 30(4): 1 DOI: 10.3969/j.issn.1009-0622.2015.04.001
    [4]
    刘怡君. 产业集群视角下有色金属供应链的优化—基于钨的分析. 生态经济, 2015, 31(11): 92 DOI: 10.3969/j.issn.1671-4407.2015.11.021

    Liu Y J. The optimization of non-Ferrous metal supply chain on the perspective of industry cluster: taking tungsten as an example. Ecol Econ, 2015, 31(11): 92 DOI: 10.3969/j.issn.1671-4407.2015.11.021
    [5]
    张保红, 牛山廷, 王玲. 特种钨合金电极材料制备工艺及组织性能研究. 粉末冶金技术, 2017, 35(4): 293 https://www.cnki.com.cn/Article/CJFDTOTAL-FMYJ201704009.htm

    Zhang B H, Niu S T, Wang L. Preparation and study on microstructure and properties of special tungsten alloy electrode material. Powder Metall Technol, 2017, 35(4): 293 https://www.cnki.com.cn/Article/CJFDTOTAL-FMYJ201704009.htm
    [6]
    赖陈, 王金淑, 周帆, 等. 新型钨铼混合基阴极的热电子发射性能. 稀有金属材料与工程, 2016, 45(7): 1871 https://www.cnki.com.cn/Article/CJFDTOTAL-COSE201607044.htm

    Lai C, Wang J S, Zhou F, et al. Thermal electron emission properties of novel W–Re mixed matrix cathodes. Rare Met Mater Eng, 2016, 45(7): 1871 https://www.cnki.com.cn/Article/CJFDTOTAL-COSE201607044.htm
    [7]
    董桂霞, 吕易楠, 韩伟丹, 等. 超级电容器电极材料的研究进展. 粉末冶金技术, 2016, 34(5): 384 DOI: 10.3969/j.issn.1001-3784.2016.05.012

    Dong G X, Lü Y N, Han W D, et al. The progress of research on electrode materials of super-capacitors. Powder Metall Technol, 2016, 34(5): 384 DOI: 10.3969/j.issn.1001-3784.2016.05.012
    [8]
    Qiu N N, Zhang Y, Zhang C, et al. Tensile properties of tungsten-rhenium wires with nanofibrous structure. Int J Miner Metall Mater, 2018, 25(9): 1055 DOI: 10.1007/s12613-018-1656-x
    [9]
    陶银龙, 方一平, 王珍珍, 等. 新形势下我国钨产业发展方向探讨. 中国矿业, 2015, 24(1): 15 https://www.cnki.com.cn/Article/CJFDTOTAL-ZGKA201501004.htm

    Tao Y L, Fang Y P, Wang Z Z, et al. Discussion on the development of tungsten industry under the new situation in China. China Min Mag, 2015, 24(1): 15 https://www.cnki.com.cn/Article/CJFDTOTAL-ZGKA201501004.htm
    [10]
    王明燕, 贾木欣, 肖仪武, 等. 中国钨矿资源现状及可持续发展对策. 有色金属工程, 2014, 4(2): 76 https://www.cnki.com.cn/Article/CJFDTOTAL-YOUS201402027.htm

    Wang M Y, Jia M X, Xiao Y W, et al. China's tungsten resources present situation and the sustainable development countermeasures. Nonferrous Met Eng, 2014, 4(2): 76 https://www.cnki.com.cn/Article/CJFDTOTAL-YOUS201402027.htm
    [11]
    Deng C, Liu S F, Ji J L, et al. Texture evolution of high purity tantalum under different rolling paths. J Mater Process Technol, 2014, 214(2): 462 DOI: 10.1016/j.jmatprotec.2013.09.026
    [12]
    Wang D Z, Hu Q W, Zeng X Y. Influences of parameters on microstructures and mechanical properties of Cr13Ni5Si2 based composite coating by laser-induction hybird cladding. Surf Coat Technol, 2015, 280: 359 DOI: 10.1016/j.surfcoat.2015.09.029
    [13]
    He L, Tan Y F, Wang X L, et al. Tribological properties of laser cladding TiB2 particles reinforced Ni-base alloy composite coatings on aluminum alloy. Rare Met, 2015, 34(11): 789 DOI: 10.1007/s12598-014-0299-y
    [14]
    Qin H, Cai Z H, Zhang P, et al. Development status of laser cladding technologies. Appl Mech Mater, 2014, 584-586: 1500 http://www.scientific.net/AMM.584-586.1500
    [15]
    Noskov A I, Gilmutdinov A Kh, Yanbaev R M. Effect of coaxial laser cladding parameters on bead formation. Int J Miner Metall Mater, 2017, 24(5): 550 http://d.wanfangdata.com.cn/Periodical/bjkjdxxb-e201705009
    [16]
    Duan H P, Liu X, Ran X Z, et al. Mechanical properties and microstructure of 3D-printed high Co–Ni secondary hardening steel fabricated by laser melting deposition. Int J Miner Metall Mater, 2017, 24(9): 1027 DOI: 10.1007/s12613-017-1492-4
  • Related Articles

    [1]Effect of solution treatment on the microstructure and properties of UNS S32750 super duplex stainless steel prepared by selective laser melting[J]. Powder Metallurgy Technology. DOI: 10.19591/j.cnki.cn11-1974/tf.2024110001
    [2]CAI Xiaoping, YIN Jinnan, ZHANG Zhipeng, FENG Peizhong. Reaction behavior, microstructure, and mechanical properties of FeAl-316 stainless steel joints[J]. Powder Metallurgy Technology, 2024, 42(2): 107-114. DOI: 10.19591/j.cnki.cn11-1974/tf.2021110009
    [3]Effects of Deoxidizing Elements Ti and La on the Microstructure and Mechanical Properties of Additively Manufactured Martensitic Stainless Steel[J]. Powder Metallurgy Technology. DOI: 10.19591/j.cnki.cn11-1974/tf.2024060018
    [4]HU Jianbin, LIU Xiaojing, WANG Zhiyong, SHANG Feng, HE Yiqiang, YANG Jianming. Microstructure and properties of 316L/430 duplex stainless steels processed by selective laser melting[J]. Powder Metallurgy Technology, 2023, 41(4): 302-306. DOI: 10.19591/j.cnki.cn11-1974/tf.2021090007
    [5]LI Jie, LIU Wen-sheng, CAI Qing-shan, DUAN You-teng, ZHU Wen-tan, MA Yun-zhu. Effect of powder characteristics on microstructure and properties of 30CrMnSiNi2A steels[J]. Powder Metallurgy Technology, 2022, 40(5): 441-450. DOI: 10.19591/j.cnki.cn11-1974/tf.2022030015
    [6]WEI Zi-chen, ZHANG Lin, QIN Ming-li, LI Xing-yu, QUE Zhong-you, QU Xuan-hui. Effect of powder size on microstructure and mechanical properties of rhenium[J]. Powder Metallurgy Technology, 2021, 39(3): 196-202. DOI: 10.19591/j.cnki.cn11-1974/tf.2021030014
    [7]WANG Xin-feng, HE Wei-wei, ZHU Ji-lei, XIANG Chang-shu. Microstructure and mechanical properties of Fe–Co–Ni based superalloy prepared by hot isostatic pressing[J]. Powder Metallurgy Technology, 2020, 38(5): 371-376, 390. DOI: 10.19591/j.cnki.cn11-1974/tf.2019060006
    [8]ZHANG Peng, WANG Zhi-yong, SHANG Feng, LI Hua-qiang, HE Yi-qiang. Effect of two phase mass ratio on the microstructure and mechanical properties of duplex stainless steel fabricated by powder metallurgy[J]. Powder Metallurgy Technology, 2020, 38(4): 269-274. DOI: 10.19591/j.cnki.cn11-1974/tf.2019060003
    [9]SUN Lu, ZHANG Ji-feng, QIU Tian-xu, SHEN Xiao-ping. Effect of forging temperature on microstructure and mechanical properties of powder hot-forged alloy contained molybdenum[J]. Powder Metallurgy Technology, 2020, 38(3): 174-182. DOI: 10.19591/j.cnki.cn11-1974/tf.2020.03.002
    [10]Tong Guoquan, Wang Erde, He Shaoyuan. THE INFLUENCE OF THE BINDER COMPOSITION ON THE MICROSTRUCTURES AND MECHANICAL PROPERTIES OF WC-20(Fe/Co/Ni) CEMENTED CARBIDES[J]. Powder Metallurgy Technology, 1995, 13(4): 243-248.
  • Cited by

    Periodical cited type(0)

    Other cited types(3)

Catalog

    Article Metrics

    Article views PDF downloads Cited by(3)
    Related

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return